Samples of approximately 10mg placed in an alumina tray and heated at a rate of 10 ℃ / min under N2 atmosphere increases, the terminal reaction temperature was 600 ℃.
The sample of about 10 mg is placed in an alumina disc and increased at a heating rate of 10 c/min in n2 atmosphere, with a terminal reaction temperature of 600 degrees C.
Put about 10mg of the sample in an alumina plate and increase it at a heating rate of 10 ℃ / min in N2 atmosphere. The terminal reaction temperature is 600 ℃.<br>