The collected PM2.5 was pretreated, the filter membrane was immersed in a beaker containing 150ml ultra pure water, and ultrasonic treatment was conducted on the ice bath for 1 hour until there was no residual PM2.5 on the filter membrane. Finally, PM2.5 flocculent particles were obtained by freezing the mixture in - 80 ° refrigerator and drying in vacuum freeze dryer.<br>
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