方法的工LOQ应在一次分析运行中评价。LOQ应通过由一个标准溶液平行制

方法的工LOQ应在一次分析运行中评价。LOQ应通过由一个标准溶液平行制备三份样品测定,此样品溶液所得峰面积的SN应约10.0,每个制备样品进样一次。峰响应应根据校正曲线计算,所测得的平均计算浓度必须在标示浓度的100.0±25.0%范围内。

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结果 (英语) 1: [复制]

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The working LOQ of the method should be evaluated in an analytical run. <br>The LOQ should be determined by preparing three samples in parallel from a standard solution, the SN of the peak area obtained from this sample solution should be about 10.0, and each sample prepared should be injected once. <br>The peak response should be calculated based on the calibration curve, and the measured average calculated concentration must be within the range of 100.0±25.0% of the labeled concentration.

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结果 (英语) 2:[复制]

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The LOQ of the method shall be evaluated in an analysis run.<br>LOQ shall be determined by preparing three samples in parallel from a standard solution. The SN of the peak area obtained from this sample solution shall be about 10.0, and each prepared sample shall be injected once.<br>The peak response shall be calculated according to the correction curve, and the measured average calculated concentration must be within 100.0 ± 25.0% of the marked concentration.

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结果 (英语) 3:[复制]

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The LOQ of the method should be evaluated in an analysis run. LOQ should be determined by preparing three samples in parallel from a standard solution, and the SN of the peak area obtained from this sample solution should be about 10.0, and each sample should be injected once. The peak response should be calculated according to the calibration curve, and the measured average calculated concentration must be within the range of 100.0 25.0% of the marked concentration.

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