采用0.1mol/L的乙酸在100℃的条件下对100nm的BaTiO3

The BaTiO3 powder with a thickness of 100 nm was hydrothermally activated with 0.1 mol/L acetic acid at 100 °C for 1 h. Then, BaTiO3 powder was cold sintered for 1 h under the conditions of 350MPa and 400℃ with Ba(OH)2·8H2O as flux. Finally, the cold sintered sample was annealed at 600 °C for 0.5 h, and a sample with a relative density of 96.62% and a grain size of 180 nm was obtained. Its normal temperature dielectric (εr) is 2836, and the dielectric loss (tanθ) is as low as 0.03.

100 nm BaTiO3 powder was hydrothermally activated with 0.1 mol / L acetic acid at 100 ℃ for 1 h. Then, BaTiO3 powder was cold sintered at 350Mpa and 400 ℃ for 1H with BA (OH) 2 · 8H2O as flux. Finally, the cold sintered samples were annealed at 600 ℃ for 0.5h, and the samples with relative density of 96.62% and grain size of 180 nm were obtained. Its normal temperature dielectric（ ε r) 2836, dielectric loss (tan) θ) As low as 0.03.

100nm BaTiO3 powder was hydrothermally activated with 0.1mol/L acetic acid at 100℃ for 1 hour. Then, BaTiO3 powder was cold sintered at 350MPa and 400℃ for 1 hour with Ba (OH) 2.8H2O as flux. Finally, the cold sintered samples were annealed at 600℃ for 0.5h, and the samples with relative density of 96.62% and grain size of 180nm were obtained. The room temperature dielectric (εr) is 2836, and the dielectric loss (tanθ) is as low as 0.03.