In this paper, ni-doped Co- Co2N heterostructures were prepared by simple thermal annealing of NiCo2O4 derived from metal-organic framework (MOF) in ammonia atmosphere, and the two-dimensional (2D) nanosheet array derived from MOF was well preserved in this process. When annealed at 350℃, the metal-metal nitride heterostructure is well formed. Figure 1 shows the detailed process of this experiment. The sample thus obtained is nitrided in ammonia water at 350℃, and the obtained sample is called Ni/Co-N-350. In the whole process, the overall shape of the two-dimensional nano-scale has been well inherited, as shown in Figure 1b.
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